{"dcterms:modified":"2025-10-10","dcterms:creator":"A Dataverse Instance","@type":"ore:ResourceMap","@id":"https://data.fz-juelich.de/api/datasets/export?exporter=OAI_ORE&persistentId=doi:10.26165/JUELICH-DATA/6RNQAR","ore:describes":{"fzj:Institute":"IET-1","Title":"Replication Data for: Electrochemical Performance and Durability of High-Temperature Solid Oxide Electrolysis Cells with SFM and SFM-GDC Fuel Electrodes for Hydrogen and Syngas Production","fzj:PoF IV topic":"Electrochemistry for Hydrogen (POF4-1231)","Author":[{"author:Name":"Wolf, Stephanie E.","author:Affiliation":"IET-1 Forschungszentrum Jülich, IPC RWTH Aachen","Identifier Scheme":"ORCID","Identifier":"0000-0002-9627-7121"},{"author:Name":"Vibhu, Vaibhav","author:Affiliation":"IET-1 Forschungszentrum Jülich","Identifier Scheme":"ORCID","Identifier":"0000-0001-9157-2722"},{"author:Name":"Chakraborty, Pritam","author:Affiliation":"IET-1 Forschungszentrum Jülich, IPC RWTH Aachen","Identifier Scheme":"ORCID","Identifier":"0000-0001-8237-3828"},{"author:Name":"Coll, Carla L.","author:Affiliation":"IET-1 Forschungszentrum Jülich"},{"author:Name":"Schönert, Sandro","author:Affiliation":"IET-1 Forschungszentrum Jülich, IPC RWTH Aachen","Identifier Scheme":"ORCID","Identifier":"0000-0001-6591-9462"},{"author:Name":"Basak, Shibabrata","author:Affiliation":"IET-1 Forschungszentrum Jülich","Identifier Scheme":"ORCID","Identifier":"0000-0002-4331-4742"},{"author:Name":"Vinke, Izaak C.","author:Affiliation":"IET-1 Forschungszentrum Jülich","Identifier Scheme":"ORCID","Identifier":"0000-0002-1361-9983"},{"author:Name":"de Haart, L.G.J. (Bert)","author:Affiliation":"IET-1 Forschungszentrum Jülich","Identifier Scheme":"ORCID","Identifier":"0000-0001-6908-1214"},{"author:Name":"Eichel, Rüdiger-A.","author:Affiliation":"IET-1 Forschungszentrum Jülich, IPC RWTH Aachen","Identifier Scheme":"ORCID","Identifier":"0000-0002-0013-6325"}],"citation:Contact":[{"datasetContact:Name":"Vibhu, Vaibhav","datasetContact:Affiliation":"IET-1","datasetContact:E-mail":"v.vibhu@fz-juelich.de"},{"datasetContact:Name":"Eichel, Rüdiger-A.","datasetContact:Affiliation":"IET-1","datasetContact:E-mail":"r.eichel@fz-juelich.de"}],"citation:Description":{"dsDescription:Text":"This data repository contains the data sets associated with the manuscript 'Electrochemical Performance and Durability of High-Temperature Solid Oxide Electrolysis Cells with SFM and SFM-GDC Fuel Electrodes for Hydrogen and Syngas Production'. Published in J. Mater. Chem. A link \r\n
\r\n\r\nMotivation:\r\nThe increasing need to valorize emitted CO2 and close the carbon cycle through the production of synthesis gas, fuel, and hydrogen has driven the development of high-temperature electrolysis technology. SOEC offers a promising solution with its ability to produce pure H2 at elevated temperatures (650°C-900°C) without the use of precious metal catalysts, making it cost-effective and more efficient than low-temperature technologies like alkaline and polymer exchange membrane cells due to advantageous kinetics and thermodynamics. By utilizing pre-existing chemical industry heat, SOEC can achieve high electrical efficiencies of up to 100%. The long-term stability and performance of current Ni-based fuel electrodes is preventing the wide industrial implementation though, prompting the search for alternative Ni-free materials with good electrochemical performance and long-term stability, such as perovskite fuel electrodes like Sr2FeMoO6-δ (SFM).\r\n
\r\nCentral Research Question:\r\nIn this work, solid oxide electrolysis cells with SFM and the composite ceramic-ceramic (cercer) SFM-GDC fuel electrode materials were investigated in steam- and co-electrolysis conditions for the first time, regarding performance and long-term stability of up to 500 h in 50% steam and 50% H2. \r\n
\r\nDescription of folder contents (switch to tree view):\r\n
\r\n01_In Situ Transmission Electron Microscopy: \r\nContains the taken TEM Images taken and the experimental procedure. \r\n\r\n02_X-Ray Diffraction_Temperature_Atmosphere Variation: \r\nContains raw data files of the XRD measurements, the TOPAS6 fit criteria, the Rietveld Report as well as the data over the whole in operando Experiment. \r\n\r\n03_X-Ray Photoelectron Spectroscopy:\r\nContains the raw data and the data evalution for the measurements in air and after reduction in H2.\r\n\r\n04_Powder_Scanning Electron Microscopy: \r\nContains the SEM Image of the unreduced and reduced sample.\r\n\r\n05_Conductivity Measurement:\r\nContains the raw data for SFM and SFM-GDC conductivty measurements in air and in H2.\r\n\r\n06_Transmission Electron Microscopy: \r\nContains the Image of one exsoluted nanoparticle observed for SFM.\r\n\r\n07_Electrochemistry_Initial Performance Characterization:\r\nContains the raw data of the initial AC and DC characterization of the cells with an SFM and an SFM-GDC fuel electrode.\r\nThe data are seperated by the operating gas atmospheres for steam electrolysis (50%H2O + 50%H2) and co-electrolysis (40%H2O + 40% CO2 + 20%H2) and then subdivided regarding the varied Parameter (Temperature, Polarization, Partial Pressure Variations).\r\n\r\n08_Electrochemistry_ResistancePlots:\r\nContains the evaluation data of the electrochemical impedance measurements for SFM and SFM-GDC.\r\n\r\n09_Electrochemistry_Degradation_Testing:\r\nContains the raw data of the electrochemical Degradation testing for SFM and SFM-GDC. \r\n\r\n10_Posttest Scanning Electron Microscopy:\r\nContains the SEM-EDS Images of the post-test characterized single cells regarding oxygen and fuel electrodes in comparison to pristine cell microstructure.\r\n\r\n11_Dilatometry:\r\nContains raw data of dilatometry measurements to analyse the thermal Expansion coefficient of SFM and SFM-GDC in air.\r\n
\r\nList of abbreviations :\r\n
\r\n AC - Alternating Current \r\n DC - Direct Current\r\n FE - Fuel Electrode\r\n OE - Oxygen Electrode\t\r\n SEM - Scanning Electron Microscopy\r\n EDS - Energy-Dispersive X-ray Spectroscopy\r\n OCV - Open Circuit Voltage"},"Subject":["Chemistry","Engineering","Physics"],"Related Publication":{"URL":"https://doi.org/10.1039/D5TA04819B"},"Contributor":[{"contributor:Type":"Data Collector","contributor:Name":"Wolf, Stephanie E."},{"contributor:Type":"Supervisor","contributor:Name":"Vibhu, Vaibhav"},{"contributor:Type":"Data Collector","contributor:Name":"Chakraborty, Pritam K."},{"contributor:Type":"Data Collector","contributor:Name":"Coll, Carla L."},{"contributor:Type":"Data Collector","contributor:Name":"Schöner, Sandro"},{"contributor:Type":"Supervisor","contributor:Name":"Basak, Shibabrata"},{"contributor:Type":"Supervisor","contributor:Name":"Vinke, Izaak C."},{"contributor:Type":"Supervisor","contributor:Name":"de Haart, L. G. J. (Bert)"},{"contributor:Type":"Supervisor","contributor:Name":"Eichel, Rüdiger-A."},{"contributor:Type":"Data Curator","contributor:Name":"Park, Junbeom"}],"Grant Information":{"grantNumber:Grant Agency":"German Federal Ministry of Education and Research (BMBF)","grantNumber:Grant Number":"FKZ 03SF0621A"},"citation:Depositor":"Park, Junbeom","Deposit Date":"2025-08-05","@id":"doi:10.26165/JUELICH-DATA/6RNQAR","@type":["ore:Aggregation","schema:Dataset"],"schema:version":"1.0","schema:datePublished":"2025-10-10","schema:name":"Replication Data for: Electrochemical Performance and Durability of High-Temperature Solid Oxide Electrolysis Cells with SFM and SFM-GDC Fuel Electrodes for Hydrogen and Syngas Production","schema:dateModified":"2025-10-10 11:57:27.375","dvcore:fileTermsOfAccess":{"dvcore:fileRequestAccess":false},"schema:includedInDataCatalog":"High-Temperature 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