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Deposition"},{"typeName":"author","multiple":true,"typeClass":"compound","value":[{"authorName":{"typeName":"authorName","multiple":false,"typeClass":"primitive","value":"Steinhoff, Michael"},"authorAffiliation":{"typeName":"authorAffiliation","multiple":false,"typeClass":"primitive","value":"IET-1 Forschungszentrum Jülich GmbH"},"authorIdentifierScheme":{"typeName":"authorIdentifierScheme","multiple":false,"typeClass":"controlledVocabulary","value":"ORCID"},"authorIdentifier":{"typeName":"authorIdentifier","multiple":false,"typeClass":"primitive","value":"0009-0008-9136-151X"}},{"authorName":{"typeName":"authorName","multiple":false,"typeClass":"primitive","value":"Domgans, Anna"},"authorAffiliation":{"typeName":"authorAffiliation","multiple":false,"typeClass":"primitive","value":"IET-1 Forschungszentrum Jülich 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Hermann"},"datasetContactAffiliation":{"typeName":"datasetContactAffiliation","multiple":false,"typeClass":"primitive","value":"IET-1 Forschungszentrum Jülich GmbH"},"datasetContactEmail":{"typeName":"datasetContactEmail","multiple":false,"typeClass":"primitive","value":"h.tempel@fz-juelich.de"}}]},{"typeName":"dsDescription","multiple":true,"typeClass":"compound","value":[{"dsDescriptionValue":{"typeName":"dsDescriptionValue","multiple":false,"typeClass":"primitive","value":"<h2>Study Overview</h2>\r\n\r\n<p>\r\nIn this study, the influence of atomic layer deposition (ALD) derived Li-Al-O interphases in garnet-type Li<sub>6.4</sub>La<sub>3</sub>Zr<sub>1.4</sub>Ta<sub>0.6</sub>O<sub>12</sub> (LLZTO) solid-state electrolyte (SSE) was investigated. Garnet-type SSE are prone to lithium dendrite growth along interfaces, which causes short-circuits, significantly reducing cell performance. ALD offers high control over coating chemistry and morphology to precisly modify these interfaces in SSEs. Here, Al<sub>2</sub>O<sub>3</sub> ALD coatings were applied on LLZTO powder. MAS NMR, XPS and STEM analysis reveal the formation of a compositionally graded Li-Al-O interphase upon deposition due to proton-exchange-induced lithium diffusion. During high-temperature sintering, the ALD coating induces densification and considerable interdiffusion with LLZTO, resulting in a multi-phase microstructure which can be directly controlled via the ALD process, as confirmed by XRD, SEM and EDS measurments. Electrochemical testing reveals that medium-thickness coatings (~ 6.8 nm,  25 ALD cycles) yield optimal performance, exhibiting ionic conductivity at room temperature of 0.39 mS/cm with good Li-dendrite resitance and long-term cycling stability.\r\n</p>\r\n\r\n<hr>\r\n\r\n<h2>Dataset Description</h2>\r\n\r\n<p>\r\nThis dataset contains NMR, XPS, XRD, Ellipsometry, EDS line scans, and electrochemical measurements to investigate Li-Al-O interphases in LLZTO.\r\n</p>\r\n\r\n<p>\r\nThe dataset is organized into the following folders:\r\n</p>\r\n\r\n<dl>\r\n\r\n<dt><strong>NMR</strong></dt>\r\n<dd>\r\n<sup>27</sup>Al Solid-state magic angle spinning nuclear magnetic resonance (MAS NMR) spectroscopy experiments were performed using an AvanceNEO spectrometer (Bruker). Data are stored in the folder <code>NMR</code>.\r\n</dd>\r\n\r\n<dt><strong>XPS</strong></dt>\r\n<dd>\r\nX-ray photoelectron spectroscopy (XPS) measurements of the Al 2p and C 1s region were conducted using a NEXSA G2 spectrometer (Thermo Fisher Scientific). Data are stored in the folder <code>XPS</code>.\r\n</dd>\r\n\r\n<dt><strong>XRD</strong></dt>\r\n<dd>\r\nX-ray diffraction (XRD) experiments were recorded using an Empyrean diffractometer (Pananalytical). Quantitative phase analysis (QPA) on the XRD diffractograms were conducted using the software package Diffrac.Topas version 7 (Bruker). The corresponding diffractograms and fitting data are stored in the folder <code>XRD</code>.\r\n</dd>\r\n\r\n<dt><strong>Ellipsometry</strong></dt>\r\n<dd>\r\nEllipsometry data were recorded using a FS-8 spectroscopic ellipsometer (Film Sense LLC). Data are stored in the folder <code>Ellipsometry</code>.\r\n</dd>\r\n\r\n<dt><strong>Electrochemistry</strong></dt>\r\n<dd>\r\nElectrochemical impedance spectroscopy (EIS), critical current density (CCD) measurements, long-term plating/stripping experiments and chronoamperometry (CA) measurements were performed. Data are stored in the folder <code>Electrochemistry</code>.\r\n</dd>\r\n\r\n<dt><strong>EDS line profile</strong></dt>\r\n<dd>\r\nEDS line profiles were recorded using a FEI Titan G2 80-200 CREWLEY system. Data are stored in the folder <code>EDS_line_profile</code>.\r\n</dd>\r\n\r\n</dl>"},"dsDescriptionDate":{"typeName":"dsDescriptionDate","multiple":false,"typeClass":"primitive","value":"2025-09-18"}}]},{"typeName":"subject","multiple":true,"typeClass":"controlledVocabulary","value":["Chemistry"]},{"typeName":"contributor","multiple":true,"typeClass":"compound","value":[{"contributorType":{"typeName":"contributorType","multiple":false,"typeClass":"controlledVocabulary","value":"Data Collector"},"contributorName":{"typeName":"contributorName","multiple":false,"typeClass":"primitive","value":"Steinhoff, Michael"}},{"contributorType":{"typeName":"contributorType","multiple":false,"typeClass":"controlledVocabulary","value":"Data Collector"},"contributorName":{"typeName":"contributorName","multiple":false,"typeClass":"primitive","value":"Domgans, Anna"}},{"contributorType":{"typeName":"contributorType","multiple":false,"typeClass":"controlledVocabulary","value":"Data 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