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Six spectra were recorded for each region of interest and averaged.\r\nAdditionally, it contains the impedance data from alternating current scanning electrochemical microscopy (AC-SECM) mapping scans (M470, BioLogic, France) of a pristine and an operated MEA anode recorded with a 10 µm Pt UME in 100 mM sulfuric acid with a 10 mV, 1 MHz AC signal at open circuit voltage.\r\n\r\n\r\nFolder contents:\r\n\r\n- Fig2_Microscopic4PP: Microscopic four-point probe data. Read the respective _README.txt file within this folder for more information.\r\n\r\n- Fig3_CrossSection: SEM cross-section images. Read the respective _README.txt file within this folder for more information.\r\n\r\n- Fig4_Raman: Microscopic Raman spectroscopy data. Read the respective _README.txt file within this folder for more information.\r\n\r\n- Fig6_AC-SECM: Raw and normalized impedance data from AC-SECM. 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