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Part 1: Document Description
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Citation |
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Title: |
Replication Data for: Electrochemical Performance and Durability of High-Temperature Solid Oxide Electrolysis Cells with SFM and SFM-GDC Fuel Electrodes for Hydrogen and Syngas Production |
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Identification Number: |
doi:10.26165/JUELICH-DATA/6RNQAR |
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Distributor: |
Jülich DATA |
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Date of Distribution: |
2025-10-10 |
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Version: |
1 |
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Bibliographic Citation: |
Wolf, Stephanie E.; Vibhu, Vaibhav; Chakraborty, Pritam; Coll, Carla L.; Schönert, Sandro; Basak, Shibabrata; Vinke, Izaak C.; de Haart, L.G.J. (Bert); Eichel, Rüdiger-A., 2025, "Replication Data for: Electrochemical Performance and Durability of High-Temperature Solid Oxide Electrolysis Cells with SFM and SFM-GDC Fuel Electrodes for Hydrogen and Syngas Production", https://doi.org/10.26165/JUELICH-DATA/6RNQAR, Jülich DATA, V1 |
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Citation |
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Title: |
Replication Data for: Electrochemical Performance and Durability of High-Temperature Solid Oxide Electrolysis Cells with SFM and SFM-GDC Fuel Electrodes for Hydrogen and Syngas Production |
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Identification Number: |
doi:10.26165/JUELICH-DATA/6RNQAR |
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Authoring Entity: |
Wolf, Stephanie E. (IET-1 Forschungszentrum Jülich, IPC RWTH Aachen) |
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Vibhu, Vaibhav (IET-1 Forschungszentrum Jülich) |
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Chakraborty, Pritam (IET-1 Forschungszentrum Jülich, IPC RWTH Aachen) |
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Coll, Carla L. (IET-1 Forschungszentrum Jülich) |
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Schönert, Sandro (IET-1 Forschungszentrum Jülich, IPC RWTH Aachen) |
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Basak, Shibabrata (IET-1 Forschungszentrum Jülich) |
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Vinke, Izaak C. (IET-1 Forschungszentrum Jülich) |
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de Haart, L.G.J. (Bert) (IET-1 Forschungszentrum Jülich) |
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Eichel, Rüdiger-A. (IET-1 Forschungszentrum Jülich, IPC RWTH Aachen) |
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Other identifications and acknowledgements: |
Wolf, Stephanie E. |
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Other identifications and acknowledgements: |
Vibhu, Vaibhav |
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Other identifications and acknowledgements: |
Chakraborty, Pritam K. |
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Other identifications and acknowledgements: |
Coll, Carla L. |
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Other identifications and acknowledgements: |
Schöner, Sandro |
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Other identifications and acknowledgements: |
Basak, Shibabrata |
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Other identifications and acknowledgements: |
Vinke, Izaak C. |
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Other identifications and acknowledgements: |
de Haart, L. G. J. (Bert) |
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Other identifications and acknowledgements: |
Eichel, Rüdiger-A. |
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Other identifications and acknowledgements: |
Park, Junbeom |
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Grant Number: |
FKZ 03SF0621A |
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Distributor: |
Jülich DATA |
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Access Authority: |
Vibhu, Vaibhav |
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Access Authority: |
Eichel, Rüdiger-A. |
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Depositor: |
Park, Junbeom |
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Date of Deposit: |
2025-08-05 |
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Study Scope |
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Keywords: |
Chemistry, Engineering, Physics |
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Abstract: |
This data repository contains the data sets associated with the manuscript <strong>'Electrochemical Performance and Durability of High-Temperature Solid Oxide Electrolysis Cells with SFM and SFM-GDC Fuel Electrodes for Hydrogen and Syngas Production'</strong>. Published in <i>J. Mater. Chem. A</i> <a href = 'https://doi.org/10.1039/D5TA04819B'> link </a> <br><br> Motivation: The increasing need to valorize emitted CO2 and close the carbon cycle through the production of synthesis gas, fuel, and hydrogen has driven the development of high-temperature electrolysis technology. SOEC offers a promising solution with its ability to produce pure H2 at elevated temperatures (650°C-900°C) without the use of precious metal catalysts, making it cost-effective and more efficient than low-temperature technologies like alkaline and polymer exchange membrane cells due to advantageous kinetics and thermodynamics. By utilizing pre-existing chemical industry heat, SOEC can achieve high electrical efficiencies of up to 100%. The long-term stability and performance of current Ni-based fuel electrodes is preventing the wide industrial implementation though, prompting the search for alternative Ni-free materials with good electrochemical performance and long-term stability, such as perovskite fuel electrodes like Sr2FeMoO6-δ (SFM). <br><br> Central Research Question: In this work, solid oxide electrolysis cells with SFM and the composite ceramic-ceramic (cercer) SFM-GDC fuel electrode materials were investigated in steam- and co-electrolysis conditions for the first time, regarding performance and long-term stability of up to 500 h in 50% steam and 50% H2. <br><br> Description of folder contents (switch to tree view): <br> <li>01_In Situ Transmission Electron Microscopy: Contains the taken TEM Images taken and the experimental procedure. </li> <li>02_X-Ray Diffraction_Temperature_Atmosphere Variation: Contains raw data files of the XRD measurements, the TOPAS6 fit criteria, the Rietveld Report as well as the data over the whole in operando Experiment. </li> <li>03_X-Ray Photoelectron Spectroscopy: Contains the raw data and the data evalution for the measurements in air and after reduction in H2.</li> <li>04_Powder_Scanning Electron Microscopy: Contains the SEM Image of the unreduced and reduced sample.</li> <li>05_Conductivity Measurement: Contains the raw data for SFM and SFM-GDC conductivty measurements in air and in H2.</li> <li>06_Transmission Electron Microscopy: Contains the Image of one exsoluted nanoparticle observed for SFM.</li> <li>07_Electrochemistry_Initial Performance Characterization: Contains the raw data of the initial AC and DC characterization of the cells with an SFM and an SFM-GDC fuel electrode. The data are seperated by the operating gas atmospheres for steam electrolysis (50%H2O + 50%H2) and co-electrolysis (40%H2O + 40% CO2 + 20%H2) and then subdivided regarding the varied Parameter (Temperature, Polarization, Partial Pressure Variations).</li> <li>08_Electrochemistry_ResistancePlots: Contains the evaluation data of the electrochemical impedance measurements for SFM and SFM-GDC.</li> <li>09_Electrochemistry_Degradation_Testing: Contains the raw data of the electrochemical Degradation testing for SFM and SFM-GDC. </li> <li>10_Posttest Scanning Electron Microscopy: Contains the SEM-EDS Images of the post-test characterized single cells regarding oxygen and fuel electrodes in comparison to pristine cell microstructure.</li> <li>11_Dilatometry: Contains raw data of dilatometry measurements to analyse the thermal Expansion coefficient of SFM and SFM-GDC in air.</li> <br> List of abbreviations : <br> <li> AC - Alternating Current </li> <li> DC - Direct Current</li> <li> FE - Fuel Electrode</li> <li> OE - Oxygen Electrode </li> <li> SEM - Scanning Electron Microscopy</li> <li> EDS - Energy-Dispersive X-ray Spectroscopy</li> <li> OCV - Open Circuit Voltage</li> |
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Methodology and Processing |
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Other Study Description Materials |
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DRT_SFM_40percH2O+40percCO2+20percH2.csv |
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WG64B_ox_HT1_900-25C.csv |
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