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This dataset provides the complete replication data supporting the publication “Ammonia Adsorption by Polyacrylonitrile-based Carbon Nanofibers (https://doi.org/10.1021/acs.iecr.6c01147)". It contains all raw and processed files required to reproduce every figure presented in the manuscript. The data is based on polyacrylonitrile-based carbon nanofiber pellet samples that were carbonized at temperatures of 800, 850, 900, 950 and 1000 °C. The dataset includes measurements by Scanning Electron Microscopy (SEM), X-Ray Photoelectron Spectroscopy (XPS) and CHNO Elemental analysis. Gas Adsorption Isotherms of Ar and CO2 were measured for general pore characterization and Monte Carlo Simulations were performed to provide Pore Size Distribution. Ammonia adsorption/desorption isotherms and adsorption equilibration curves were measured at 25 and 50 °C.

Methods:
All methods and post-processing procedures are available under https://doi.org/10.1021/acs.iecr.6c01147


Folder Structure:
- Measurement Type
- Raw Data Files
- Metadata Files with explanation to technical measurement details

Sample Name : PAN - CXXX (Polyacrylonitrile - Carbonization Temperature)


Abbreviations:

PAN = Polyacrylonitrile
SEM = Scanning Electron Microscopy
XPS = X-Ray Photoelectron Spectroscopy
Ar = Argon
CO2 = Carbondioxide
NH3 = Ammonia
PSD = Poresize Distribution
SEQ = Static Equilibration Curve


Relationship of data:
Raw data, metadata for measurement


Relationship of data and figures in paper:

Main text:
figure 1 = SEM
figure 2 = CHNO
figure 3 = XPS
figure 4 = Adsorption - Ar - Isotherms
figure 5 = Adsorption - CO2 - Isotherms, PSD
figure 6 = Adsorption - NH3 - Isotherms - 298K, 323K
figure 7 = Adsorption - NH3 - Isotherms - 298K, 303K, 308K, 323K
figure 8 = calculated from data in figure 7
figure 9 = Adsorption - NH3 - Equilibration Curves - 298K, 323K
figure 10 = calculated from fit fuctions in figure 9

Supporting Information:
figure 1 = XPS
figure 2 = XPS
figure 3 = Adsorption - NH3 - Isotherms - 298K, 303K, 308K, 323K
figure 4 = Adsorption - NH3 - SEQ - Measurements - 298K-50mbar, 298K-100mbar, 323K-50mbar, 323K-100mbar
figure 5 = Adsorption - NH3 - SEQ - Measurements - 298K-50mbar, 298K-100mbar, 323K-50mbar, 323K-100mbar
figure 6 = Adsorption - NH3 - SEQ - Measurements - 298K-50mbar, 298K-100mbar, 323K-50mbar, 323K-100mbar